Annual Reports in Inorganic and General Syntheses–1974 by Kurt Niedenzu

By Kurt Niedenzu

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503 (1974). F. Rendle, A. Storr and J. Trotter, J. CHEM. , 2252 (1973). K. V. Saraev, C M . G. V. Mironova, IZV. AKAD. NAUK. SSSR, Ser. , 2136 (1974) . w · Kaminsky, J · Kopf and C Thirase, JUSTUS LIEBIGS ANN. CHEM. , 9_, 1531 (1974) . A. Kovar, C Loaris, H. O. Callaway, INORG. , 13, 1476 (1974). S. J. Worall, J. , 81,, 329 (1974) . G. J. Worall, J. ORGANOMETAL. L, 23 (1974) . L. Atwood, D . R. Newberry, CRYST. STRUCT. , 3^, 6 1 5 (1974). L. R. , 66_, 15 (1974) . L. Wilson and K. CHEM. , 61_, 229 (1974) .

K. Sen, T. B. Brennan, and H. Gilman, J. INDIAN CHEM. SOC. , 5_1, 561 (1974) . 54. P. Mazerolles, M. Joanny and G. Tourrou, J. ORGANOMETAL. , M ) , C3 (1973). 55. L. Birkofer and W. Weniger, CHEM. , 106, 3595 (1973). 56. F. P. Tsui and G. Zon, J. ORGANOMETAL. , 7Ό> C3 (1974). 57. H. Sakurai, Y. Kobayashi, and Y. Nakadaira, J. AMER. CHEM. SOC. 6, 2656 (1974) . 58. R. Calas, J. Dunogues and G. Deleris, J. ORGANOMETAL. , 7±9 371 (1974) . 59. W. H. Atwell and G. N. Bokerman, Fr. Demande, 2,163,579.

Higher yields of HC=C(Me), I 7 Si(Me) 2 «AAV Me2SiCl2 Mg ~(50-60°) HMPT or THF A (2) Me Me (40-60%) cyclic product were reported for reaction of hexatriene in the 40 ANNUAL REPORTS IN INORGANIC AND GENERAL SYNTHESES 1974 presence of Cu^Cl^ (26). The effect of solvent on the ring closure reaction has also been studied (27). Previous methods employed Na/THF and produced lower yields of the silacyclopentene . In contrast to other routes which require low temperatures partial silylation of gem-polychlor inated compounds with Me SiCl/Mg/HMPT can be accomplished under mild conditions (3060 , 15 to 40 hours) to give 10 to 80% yields of coupled product (29) .

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